The batch distillation process has existed for many centuries. It is perhaps the oldest technology for separating or purifying liquid mixtures and is the most frequently used separation method in batch processes. In the last 25 years, with continuous development of faster computers and sophisticated numerical methods, there have been many published works using detailed mathematical models with rigorous physical property calculations and advanced optimisation techniques to address several important issues, such as selection of column configurations, design, operation, off-cut recycling, use of batch distillation in reactive and extractive modes, etc.Batch Distillation: Design and Operation presents excellent, important contributions of many researchers from around the globe, including those of the author and his co-workers./a
Three important areas of process dynamics and control: chemical reactors, distillation columns and batch processes are the main topics of discussion and evaluation at the IFAC Symposium on Dynamics and Control of Chemical Reactors, Distillation Columns and Batch Processes (DYCORD '95). This valuable publication was produced from the latest in the series, providing a detailed assessment of developments of key technologies within the field of process dynamics and control.
This volume presents reports from the 1997 conference, held in Maastricht, Netherlands. The papers, covering a broad range of topics from the estimation of physical properties to the design and performance of contacting trays, demonstrate the high rate of advance in technology.
This book presents a detailed and practical description of various processes – dewatering, desalting, and distillation – that prepare refinery feedstocks for different conversion processes they will go through. Relevant process data are provided, and process operations are fully described. This accessible guide is written for managers, professionals, and technicians as well as graduate students transitioning into the refining industry. Key Features: • Describes feedstock evaluation and the effects of elemental, chemical, and fractional composition. • Details the equipment and components and possible impacts due to composition. • Explores the process options and parameters involved in dewatering, desalting, and distillation. • Considers next-generation processes and developments.
Most available books in chemical engineering mainly pertain to continuous processes, with batch distillation relegated to a small section. Filling this void in the chemical engineering literature, Batch Distillation: Simulation, Optimal Design, and Control, Second Edition helps readers gain a solid, hands-on background in batch processing. The second edition of this bestseller explores numerous new developments in batch distillation that have emerged since the publication of the first edition. New to the Second Edition Special sections on complex column configurations and azeotropic, extractive, and reactive distillation A chapter on various kinds of uncertainties in batch distillation A chapter covering software packages for batch distillation simulation, design, optimization, and control Separate chapters on complex columns and complex systems Up-to-date references and coverage of recent research articles This edition continues to explain how to effectively design, synthesize, and make operations decisions related to batch processes. Through careful treatments of uncertainty analysis, optimization, and optimal control methods, the author gives readers the necessary tools for making the best decisions in practice. While primarily designed for a graduate course in batch distillation, the text can also be used in undergraduate chemical engineering courses. In addition, researchers and academics faced with batch distillation research problems and practicing chemical engineers tackling problems in actual day-to-day operations will find the book to be a useful reference source.
Distillation: Operation and Applications—winner of the 2015 PROSE Award in Chemistry & Physics from the Association of American Publishers—is a single source of authoritative information on all aspects of the theory and practice of modern distillation, suitable for advanced students and professionals working in a laboratory, industrial plants, or a managerial capacity. It addresses the most important and current research on industrial distillation, including all steps in process design (feasibility study, modeling, and experimental validation), together with operation and control aspects. This volume features an extra focus on distillation applications. Winner of the 2015 PROSE Award in Chemistry & Physics from the Association of American Publishers Practical information on the newest development written by recognized experts Coverage of a huge range of laboratory and industrial distillation approaches Extensive references for each chapter facilitates further study
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Distillation has historically been the main method forseparating mixtures in the chemical process industry. However,despite the flexibility and widespread use of distillationprocesses, they still remain extremely energy inefficient.Increased optimization and novel distillation concepts can deliversubstantial benefits, not just in terms of significantly lowerenergy use, but also in reducing capital investment and improvingeco-efficiency. While likely to remain the separation technology ofchoice for the next few decades, there is no doubt thatdistillation technologies need to make radical changes in order tomeet the demands of the energy-conscious society. Advanced Distillation Technologies: Design, Control andApplications gives a deep and broad insight into integratedseparations using non-conventional arrangements, including bothcurrent and upcoming process intensification technologies. It includes: Key concepts in distillation technology Principles of design, control, sizing and economics ofdistillation Dividing-wall column (DWC) – design, configurations,optimal operation and energy efficient and advanced control DWC applications in ternary separations, azeotropic, extractiveand reactive distillation Heat integrated distillation column (HIDiC) – design,equipment and configurations Heat-pump assisted applications (MVR, TVR, AHP, CHRP, TAHP andothers) Cyclic distillation technology – concepts, modelingapproach, design and control issues Reactive distillation – fundamentals, equipment,applications, feasibility scheme Results of rigorous simulations in Mathworks Matlab &Simulink, Aspen Plus, Dynamics and Custom Modeler Containing abundant examples and industrial case studies, thisis a unique resource that tackles the most advanced distillationtechnologies – all the way from the conceptual design topractical implementation. The author of Advanced Distillation Technologies, Dr. Ir.Anton A. Kiss, has been awarded the Hoogewerff Jongerenprijs2013. ahref="http://www.hoogewerff-fonds.nl/nieuws/26/hoogewerff_jongerenprijs_2013_toegekend_aan_veelzijdige_procestechnoloog"Findout more (website in Dutch).../a
While most wine and spirits books focus on vineyard and crop management or fermentation and distillation processes, few address critical post process aspects of stabilization, aging, and spoilage. This book serves as a comprehensive source of information on post-fermentation and -distillation technology applied to wine, beer, vinegar and distillates in a broad spectrum. Post-Fermentation and -Distillation Technology: Stabilization, Aging, and Spoilage thoroughly describes all of the operations related to these products after the fermentation or distillation steps, focusing on the complex issues related to their stabilization, aging, and spoilage. The final product must be stable against microbial activity as well as undesirable chemical and physical chemical reactions that occur in the bottle. For example, clarity, stability, compositional adjustment, style development and packaging represent the five goals of "finishing" a wine. Concerning the visual defects associated with spoilage, it is crucial that wine at the point of consumption not be cloudy or contain any haze or precipitate, especially white wines. Similarly, it is also important to prevent unwanted microbial growth from occurring in the wine after the primary fermentation is complete, affecting the flavor and aroma profile in unpredicted ways. The book addresses all of these issues and more. Moreover, the discussion also involves beer, vinegar and distillates, giving this book a novel and interesting approach. The book combines referenced research with practical applications and case studies of novel technologies such as square barrels, synthetic closures, and Tetra Pak®.
Contains the papers presented at a symposium which aimed to address and record changes in distillation and absorption and to discuss new directions. Topics covered include: column sequencing; equipment; batch distillation; azeotropic and extractive distillation; packed columns and more.
These volumes are part of Encyclopedia of Water Sciences, Engineering and Technology Resources in the global Encyclopedia of Life Support Systems (EOLSS), which is an integrated compendium of twenty one Encyclopedias. The three volumes present state-of-the art subject matter of various aspects of Common Fundamentals and Unit Operations in Thermal Desalination Systems such as: Conventional Water Treatment Technologies; Guidelines for Potable Water Purification; Advanced Treatment Technologies for Recycle - Reuse of Domestic Wastewater; Composition of Desalinated Water; Crystallization; Deep Bed Filtration: Modeling Theory and Practice; Distillation ; Rectification; Flocculation and Flocculation Filtration; Hazardous Waste Treatment Technologies; Microfiltration and Ultrafiltration; Post-Treatment of Distillate and Permeate; Pre-Cleaning Measures: Filtration; Raw Water Pre-Treatment: Sludge Treatment Technologies; Supercritical Extraction; Potential for Industrial Wastewater Reuse; Treatment of Industrial Wastewater by Membrane Bioreactors; Unconventional Sources of Water Supply; Problem of Non-Condensable Gas Release in Evaporators; Entrainment in Evaporators; Mist Eliminators; Chemical Hazards in Seawater Desalination by the Multistage-Flash Evaporation Technique; Concentration of Liquid Foods; Environmental Impact of Seawater Desalination Plants; Environmental Impacts of Intakes and Out Falls; Industrial Ecology, Water Resources, and Desalination; Rural and Urban Water Supply and Sanitation; Sustainable Development, Water Supply and Sanitation Technology These volumes are aimed at the following five major target audiences: University and College Students Educators, Professional Practitioners, Research Personnel and Policy and Decision Makers.